Determination of ultra-trace Pt, Pd and Rh in seawater using an off-line pre-concentration method and inductively coupled plasma mass spectrometry
Liu, Kai; Gao, Xuelu; Li, Li; Chen, Chen-Tung Arthur; Xing, Qianguo
Source PublicationCHEMOSPHERE
ISSN0045-6535
2018-12
Volume212Pages:429-437
KeywordPlatinum group elements Seawater ICP-MS Pre-concentration Chelating resin
MOST Discipline CatalogueEnvironmental Sciences & Ecology
DOI10.1016/j.chemosphere.2018.08.098
Contribution Rank[Liu, Kai; Gao, Xuelu; Xing, Qianguo] Chinese Acad Sci, Yantai Inst Coastal Zone Res, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Yantai 264003, Peoples R China; [Liu, Kai; Gao, Xuelu] Univ Chinese Acad Sci, Beijing 100049, Peoples R China; [Li, Li] State Ocean Adm, Inst Oceanog 1, Qingdao 266601, Shandong, Peoples R China; [Chen, Chen-Tung Arthur] Natl Sun Yat Sen Univ, Dept Oceanog, Kaohsiung 80424, Taiwan
Department海岸带信息集成与综合管理实验室
AbstractA method was modified for the preconcentration of platinum (Pt), palladium (Pd) and rhodium (Rh) from seawater by a solid phase extraction using a commercially available resin Nobias-chelate PA1 (R). All the determination was conducted using inductively coupled plasma mass spectrometry (ICP-MS) which had a low detection limit for Pt, Pd and Rh, about 16.53,16.41 and 26.88 pg L-1, respectively. It was found that the adsorption performance of the resin was closely related to the matrix, ligands and pH of the samples. Significant difference in recovery was found in various samples: seawater approximate to artificial seawater > ultra pure deionized water. This method had low method blank in the range of 5.51-8.89 pg L-1 and high enrichment factor of up to 180-200. The recoveries of Pt and Pd were 93 +/- 4.2% in the spiked real seawater. However, the recovery of Rh on the resin was below 70% but stable in the range of 65-68%. It indicated that the Rh recovery seemed to be reproducible and higher volumes of seawater must be processed in order to obtain the lower limit of quantification and excellent recovery. (C) 2018 Elsevier Ltd. All rights reserved.
SubtypeArticle
Indexed BySCI
Language英语
WOS KeywordPLATINUM-GROUP ELEMENTS ; CATHODIC STRIPPING VOLTAMMETRY ; CHEMICAL-VAPOR GENERATION ; RARE-EARTH-ELEMENTS ; ICP-MS ; SPECTRAL INTERFERENCES ; DISSOLVED PLATINUM ; MARINE MACROALGA ; CHELATING RESIN ; FLOW-INJECTION
WOS Research AreaEnvironmental Sciences
WOS IDWOS:000447478100047
Funding OrganizationNational Natural Science Foundation of China [41376083] ; Aoshan Technology Innovation Program of the Qingdao National Laboratory for Marine Science and Technology [2016ASKJ02-4] ; Strategic Priority Research Program of the Chinese Academy of Sciences [XDA11020702, XDA11020305]
Citation statistics
Cited Times:11[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.yic.ac.cn/handle/133337/24583
Collection中科院海岸带环境过程与生态修复重点实验室_海岸带信息集成与战略规划研究中心
Affiliation1.Chinese Acad Sci, Yantai Inst Coastal Zone Res, CAS Key Lab Coastal Environm Proc & Ecol Remediat, Yantai 264003, Peoples R China;
2.Univ Chinese Acad Sci, Beijing 100049, Peoples R China;
3.State Ocean Adm, Inst Oceanog 1, Qingdao 266601, Shandong, Peoples R China;
4.Natl Sun Yat Sen Univ, Dept Oceanog, Kaohsiung 80424, Taiwan
Recommended Citation
GB/T 7714
Liu, Kai,Gao, Xuelu,Li, Li,et al. Determination of ultra-trace Pt, Pd and Rh in seawater using an off-line pre-concentration method and inductively coupled plasma mass spectrometry[J]. CHEMOSPHERE,2018,212:429-437.
APA Liu, Kai,Gao, Xuelu,Li, Li,Chen, Chen-Tung Arthur,&Xing, Qianguo.(2018).Determination of ultra-trace Pt, Pd and Rh in seawater using an off-line pre-concentration method and inductively coupled plasma mass spectrometry.CHEMOSPHERE,212,429-437.
MLA Liu, Kai,et al."Determination of ultra-trace Pt, Pd and Rh in seawater using an off-line pre-concentration method and inductively coupled plasma mass spectrometry".CHEMOSPHERE 212(2018):429-437.
Files in This Item: Download All
File Name/Size DocType Version Access License
Determination of ult(789KB)期刊论文出版稿开放获取CC BY-NC-SAView Download
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Liu, Kai]'s Articles
[Gao, Xuelu]'s Articles
[Li, Li]'s Articles
Baidu academic
Similar articles in Baidu academic
[Liu, Kai]'s Articles
[Gao, Xuelu]'s Articles
[Li, Li]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Liu, Kai]'s Articles
[Gao, Xuelu]'s Articles
[Li, Li]'s Articles
Terms of Use
No data!
Social Bookmark/Share
File name: Determination of ultra-trace Pt, Pd and Rh in seawater using an off-line pre-concentration method and inductively coupled plasma mass spectrometry.pdf
Format: Adobe PDF
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.