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一种6-氨基-6-脱氧菊糖及其制备和应用
郭占勇; 任剑明; 董方; 冯艳; 彭德金
Rights Holder中国科学院烟台海岸带研究所
2010-11-22
Status有效-授权
Country山东(37)
Abstract本发明涉及日化领域及医药行业,具体讲是一种6-氨基-6-脱氧菊糖及其制备和应用。6-氨基-6-脱氧菊糖为式(1)所示,其中n的平均取值范围是10-35。制备将菊糖经卤代反应或菊糖与磺酰氯酯化,菊糖卤代或酯化得产物分别与叠氮钠或叠氮锂在40-70℃条件下反应8-24h,即均得到6-叠氮-6-脱氧菊糖,将6-叠氮-6-脱氧菊糖经三苯基膦或氢化铝锂还原,即得到6-氨基-6-脱氧菊糖;本发明通过有效的合成手段得到的6-氨基-6-脱氧菊糖,使用卤素取代菊糖的伯羟基或磺酰氯与菊糖成酯造成菊糖六位易离去集团,叠氮基亲核取代并经还原后得取高代度的6-氨基-6-脱氧菊糖。本发明合成步骤简单,易于推广,所需设备及原料易得。式(1)
Subject AreaC08b37/18 ; A61k31/733 ; A61p39/06
URL查看原文
Application NumberCN201010570421.X
Open (Notice) NumberCN102060942A
Language中文
PCT Attributes
Document Type专利
Identifierhttp://ir.yic.ac.cn/handle/133337/22129
Collection海岸带生物学与生物资源利用所重点实验室
Affiliation中国科学院烟台海岸带研究所
Recommended Citation
GB/T 7714
郭占勇,任剑明,董方,等. 一种6-氨基-6-脱氧菊糖及其制备和应用[P]. 2010-11-22.
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