Institutional Repository of Key Laboratory of Coastal Zone Environmental Processes, Yantai Institute of Coastal Zone Research, Chinese Academy of Sciences (KLCEP)
C-18-Functionalized Magnetic Silica Nanoparticles for Solid Phase Extraction of Microcystin-LR in Reservoir Water Samples Followed by HPLC-DAD Determination | |
Ma, Jiping; Yan, Fengli; Chen, Fengxi; Jiang, Lianhua; Li, Jinhua; Chen, Lingxin; Ma, JP (reprint author), Qingdao Technol Univ, Sch Environm & Municipal Engn, Key Lab Environm Engn Shandong Prov, Qingdao 266033, Peoples R China. majiping2012@163.com | |
发表期刊 | JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES |
ISSN | 1082-6076 |
2015-04-03 | |
卷号 | 38期号:6页码:655-661 |
关键词 | Microcystins Preconcentration C-18-functionalized Magnetic Silica Nanoparticles Hplc-dad Magnetic Solid Phase Extraction Water Samples |
DOI | 10.1080/10826076.2014.936611 |
产权排序 | [Ma, Jiping; Yan, Fengli; Jiang, Lianhua] Qingdao Technol Univ, Sch Environm & Municipal Engn, Key Lab Environm Engn Shandong Prov, Qingdao 266033, Peoples R China; [Chen, Fengxi] Wuhan Inst Technol, Sch Chem Engn & Pharm, Wuhan, Peoples R China; [Li, Jinhua; Chen, Lingxin] Chinese Acad Sci, Yantai Inst Coastal Zone Res, Key Lab Coastal Environm Proc & Ecol Remediat, Yantai, Peoples R China |
作者部门 | 中科院海岸带环境过程与生态修复重点实验室 |
英文摘要 | In this study, C-18-functionalized magnetic silica nanoparticle (Fe3O4@SiO2@C-18 MNPs) based magnetic solid phase extraction (MSPE) was successfully developed for the determination of microcystin-LR (MC-LR) in reservoir water samples followed by high performance liquid chromatography-diode array detection (HPLC-DAD). After the extraction, the adsorbent can be conveniently and rapidly separated from aqueous samples by an external magnet. The main factors influencing the extraction efficiency including the amount of the MNPs, the extraction time, the pH of sample solution, and desorption conditions were optimized to obtain high recoveries and extraction efficiency. High enrichment factor 500 was attained. Under the optimized experimental conditions, the calibration curve of MC-LR was linear in the range of 0.1-10.0 mu g/L with correlation coefficients (r(2)) 0.9996. Limit of detection (LOD, S/N=3) of the method was 0.056 mu g/L. The developed method was successfully applied to the determination of MC-LR in reservoir water samples. The method recoveries were obtained ranging from 73.3-104% for three spiked concentrations, with the relative standard deviations (RSD) of 2.90-4.30%. The developed Fe3O4@SiO2@C-18 MNPs-based MSPE coupled with HPLC-DAD demonstrated excellent sensitivity and repeatability, simplicity, rapidity, and ease of operation, as well as practical applicability. |
文章类型 | 期刊论文 |
资助机构 | Biochemistry & Molecular Biology ; Chemistry |
收录类别 | SCI |
语种 | 英语 |
关键词[WOS] | PERFORMANCE LIQUID-CHROMATOGRAPHY ; POLYCYCLIC AROMATIC-HYDROCARBONS ; CLOUD-POINT EXTRACTION ; MASS-SPECTROMETRY ; ENVIRONMENTAL WATER ; NATURAL-WATERS ; ALGAL TOXINS ; MICROEXTRACTION ; PRECONCENTRATION ; DERIVATIZATION |
研究领域[WOS] | National Natural Science Foundation of China [21107057, 51078193] ; Natural Science Foundation of Shandong Province [ZR2010BL024] ; Taishan Scholar Construction Project Special Foundation [2010016010] ; Special Foundation of Central Financial Support to Local Colleges and Universities [201020029] |
WOS记录号 | WOS:000347786800001 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.yic.ac.cn/handle/133337/8633 |
专题 | 中国科学院海岸带环境过程与生态修复重点实验室 |
通讯作者 | Ma, JP (reprint author), Qingdao Technol Univ, Sch Environm & Municipal Engn, Key Lab Environm Engn Shandong Prov, Qingdao 266033, Peoples R China. majiping2012@163.com |
推荐引用方式 GB/T 7714 | Ma, Jiping,Yan, Fengli,Chen, Fengxi,et al. C-18-Functionalized Magnetic Silica Nanoparticles for Solid Phase Extraction of Microcystin-LR in Reservoir Water Samples Followed by HPLC-DAD Determination[J]. JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,2015,38(6):655-661. |
APA | Ma, Jiping.,Yan, Fengli.,Chen, Fengxi.,Jiang, Lianhua.,Li, Jinhua.,...&Ma, JP .(2015).C-18-Functionalized Magnetic Silica Nanoparticles for Solid Phase Extraction of Microcystin-LR in Reservoir Water Samples Followed by HPLC-DAD Determination.JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES,38(6),655-661. |
MLA | Ma, Jiping,et al."C-18-Functionalized Magnetic Silica Nanoparticles for Solid Phase Extraction of Microcystin-LR in Reservoir Water Samples Followed by HPLC-DAD Determination".JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES 38.6(2015):655-661. |
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