Synthesis of MoS2 nanoparticles using MoO3 nanobelts as precursor via a PVP-assisted hydrothermal method | |
Zeng, XZ; Qin, W; Qin, W (reprint author), Chinese Acad Sci, Yantai Inst Coastal Zone Res YIC, Key Lab Coastal Environm Processes & Ecol Remedia, Yantai 264003, Shandong, Peoples R China.; Qin, W (reprint author), YICCAS, Shandong Prov Key Lab Coastal Environm Processes, Yantai 264003, Shandong, Peoples R China. Email:wqin@yic.ac.cn | |
发表期刊 | MATERIALS LETTERS |
ISSN | 0167-577X |
2016-11-01 | |
卷号 | 182页码:347-350 |
关键词 | Mos2 Nanoparticles Moo3 Nanobelts Surfactant Assistance Semiconductors |
DOI | 10.1016/j.matlet.2016.07.026 |
产权排序 | [Zeng, Xianzhong; Qin, Wei] Chinese Acad Sci, Yantai Inst Coastal Zone Res YIC, Key Lab Coastal Environm Processes & Ecol Remedia, Yantai 264003, Shandong, Peoples R China; [Zeng, Xianzhong; Qin, Wei] YICCAS, Shandong Prov Key Lab Coastal Environm Processes, Yantai 264003, Shandong, Peoples R China; [Zeng, Xianzhong] Univ Chinese Acad Sci, Beijing 100039, Peoples R China |
作者部门 | 中科院海岸带环境过程与生态修复重点实验室 |
英文摘要 | The synthesis of MoS2 nanoparticles from MoO3 with a certain morphology through a surfactant-assisted hydrothermal process is described in this paper. MoO3, which has a nanobelt morphology with a width of 100-500 nm and a length from one to several micrometers, is used as the precursor, and poly(vinylpyrrolidone) (PVP) is used as the surfactant. The morphology of the resulting MoS2 nanomaterial has been characterized by the field-emission scanning electron microscope, which shows that the obtained nanoparticles have diameters ranging from 50 to 100 nm with rough surfaces. Additionally, the composition and crystallinity as well as the phase information of the produced nanoparticles have been characterized by the energy-dispersive X-ray spectrometer and X-ray diffraction. Specifically, in this process, the presence of PVP plays a crucial role for the successful fabrication of the nanoparticle morphology, which may be due to the formation of PVP micelles leading to an oriented aggregation of MoS2 nuclei. In addition, comparative experiments have been conducted and the possible reaction mechanism is proposed. (C) 2016 Elsevier B.V. All rights reserved. |
文章类型 | Article |
资助机构 | Strategic Priority Research Program of the Chinese Academy of Sciences(XDA11020702) ; National Natural Science Foundation of China(21475148) ; Taishan Scholar Program of Shandong Province(TS20081159) |
收录类别 | SCI |
语种 | 英语 |
关键词[WOS] | FULLERENE-LIKE NANOPARTICLES ; SINGLE-LAYER MOS2 ; MICROSPHERES ; NANOTUBES ; NANORODS ; CATALYST ; GAS |
研究领域[WOS] | Materials Science ; Physics |
WOS记录号 | WOS:000382338400085 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.yic.ac.cn/handle/133337/17241 |
专题 | 海岸带生物学与生物资源利用重点实验室_海岸带生物学与生物资源保护实验室 |
通讯作者 | Qin, W (reprint author), Chinese Acad Sci, Yantai Inst Coastal Zone Res YIC, Key Lab Coastal Environm Processes & Ecol Remedia, Yantai 264003, Shandong, Peoples R China.; Qin, W (reprint author), YICCAS, Shandong Prov Key Lab Coastal Environm Processes, Yantai 264003, Shandong, Peoples R China. Email:wqin@yic.ac.cn |
推荐引用方式 GB/T 7714 | Zeng, XZ,Qin, W,Qin, W ,et al. Synthesis of MoS2 nanoparticles using MoO3 nanobelts as precursor via a PVP-assisted hydrothermal method[J]. MATERIALS LETTERS,2016,182:347-350. |
APA | Zeng, XZ,Qin, W,Qin, W ,&Qin, W .(2016).Synthesis of MoS2 nanoparticles using MoO3 nanobelts as precursor via a PVP-assisted hydrothermal method.MATERIALS LETTERS,182,347-350. |
MLA | Zeng, XZ,et al."Synthesis of MoS2 nanoparticles using MoO3 nanobelts as precursor via a PVP-assisted hydrothermal method".MATERIALS LETTERS 182(2016):347-350. |
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